Ok this generic advice as I am not 'up' on a 4400
To the greatest extent possible, you wish to leave both the card and the switch port on autonegotiate. this is the mose reliable mode, as they can switch down in bad times.
If you need to switch either the card or the port to a fixed setting, then you MUST switch both. Auto negotiate makes horrible choices if one side won't autonegotiate.
I sometimes find that the card/port cannot go 100 on an older wire, (my wireplant dates to 1992) but 10full does work. more rarely, I find 3com PC cards were the 10 meg does not work at all, just 100, no idea why. be kind to yourself and mark these wires! one generation of Lexmark laser printers thought they could do 10/100 but would only do 10.
I tried to remain child-like, all I acheived was childish.